Microdosage de l'isoniazide et de l'acetylisoniazide plasmatiques par chromatographie liquide à haute performance
Identifieur interne : 001641 ( France/Analysis ); précédent : 001640; suivant : 001642Microdosage de l'isoniazide et de l'acetylisoniazide plasmatiques par chromatographie liquide à haute performance
Auteurs : C. Lacroix [France] ; G. Laine [France] ; J. P. Goulle [France] ; J. Nouveau [France]Source :
- Journal of Chromatography B: Biomedical Sciences and Applications [ 0378-4347 ] ; 1984.
Abstract
Abstract: Determination of isoniazid and acetylisoniazid in plasma or serum by high-performance liquid chromatographyA method for the analysis of iosoniazid and acetylisoniazid in plasma or serum has been developed. This report describes a simple, quick and economically optimized reversed-phase high-performance liquid chromatographic assay using a small sample size without solvent extraction step. Isoniazid was condensed with cinnamic aldehyde after trichloroacetic acid deproteinisation. The method correlated well with a fluorimetric procedure. Precision, sensibility and accuracy were good. Common antituberculous drugs did not interfere.
Url:
DOI: 10.1016/S0378-4347(00)84080-3
Affiliations:
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This report describes a simple, quick and economically optimized reversed-phase high-performance liquid chromatographic assay using a small sample size without solvent extraction step. Isoniazid was condensed with cinnamic aldehyde after trichloroacetic acid deproteinisation. The method correlated well with a fluorimetric procedure. Precision, sensibility and accuracy were good. Common antituberculous drugs did not interfere.</div></front></TEI><affiliations><list><country><li>France</li></country></list><tree><country name="France"><noRegion><name sortKey="Lacroix, C" sort="Lacroix, C" uniqKey="Lacroix C" first="C." last="Lacroix">C. Lacroix</name></noRegion><name sortKey="Goulle, J P" sort="Goulle, J P" uniqKey="Goulle J" first="J. P." last="Goulle">J. P. Goulle</name><name sortKey="Laine, G" sort="Laine, G" uniqKey="Laine G" first="G." last="Laine">G. Laine</name><name sortKey="Nouveau, J" sort="Nouveau, J" uniqKey="Nouveau J" first="J." last="Nouveau">J. 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